Design Recommendations
As mentioned before,
the green part (before sintering) is produced by either compaction
of powder or injection molding. Those stages restrict the shapes
and kinds of parts the user can design. When injection molding is
used, the designer should follow the good practices mentioned in
the metal/ceramic injection molding design
guide.
When compaction is used,
the designer should take into account the following. During compaction
of the part, pressure is applied equally from above and below to
the powder being compacted. The powder is comtained in a die. Due
to the irregular shape of the powder particles employed, the powders
interlock mechanically and become a coherent mass. This interlocking
characteristic will forbid the powder from flowing under pressure
as plastic material would flow during molding. Hence the importance
of designing the component such that the powder can be conformed
to the required shape during filling and before pressing commences.
The removal of volatile
materials, if present in appreciable quantities in the compacts,
will produce a porous and permeable product. The designer should
take advantage of this feature in designing products such as metal
filters.
We mention some general
design guides that fall in the category of designing of the manufacturing
line:
- In the first stage in the furnace, the temperature of the compacts
should be raised in a controlled manner. Air and volatilizing
liquids entrapped in closed pores during rapid heating produce
high internal pressure. This would result in swelling or fracture
of the compacts.
- The time during the second stage of sintering must be sufficient
to produce the desired density and final properties.
- Reduced atmospheres are preferred. They can reduce any oxide
already present on the particle surfaces and combust harmful gases
that are liberated during the sintering. For sintering a variety
of other metals, the most commonly used gases are hydrogen, dissociated
or burned ammonia, partially combusted hydrocarbon gases, and
nitrogen.
- To control the carburization and decarburization of iron and
iron-base compacts and to prevent oxidation of powders, an oxygen-free
atmosphere is needed.
- A vacuum is generally
used for sintering refractory metal alloys and stainless steels.
- As the temperature increases in the furnace, and bonding by
diffusion occurs between adjacent particles, the strength, density,
ductillity, and thermal and electrical conductivities of the compact
increase while the compact shrinks; therefore allowances should
be made for shrinkage
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